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Bensellam, M., Laybutt, D

Once again, I want to be very clear that the FDA has not approved the use of these drugs but they have moved them into a different category so they can actually be compounded

HPLC grade acetonitrile (ACN), acetic acid and water, and reagent grade trifluoroacetic acid (TFA) were purchased from Sigma/Aldrich (St Louis, MO)

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This is because endotoxins may introduce unwanted variables into laboratory studies and cause biological contamination, affecting experimental reproducibility